The F-30 single-layer glass reactor can be subjected to vacuum stirring reaction, distillation concentration reaction, heat generation (exothermic reaction), etc.
A:(Only for reactors below 5L, more than 5L are equipped with special personnel)
1 After unpacking, check that the main accessories of the unit are complete according to the packing list.
2. Assemble the frame in accordance with the drawings as shown in the figure.
3. Install the electrical box on the top of the right rear pole and tighten the screws and insert the seven-pin plug. Install the vacuum gauge on the left rear end and tighten the screws.
4. According to the height of use, fix the round bracket of the kettle to the vertical pole slider, and place the kettle on the bracket. The semi-circular hoop is used to insert the pole of the kettle into the pole of the kettle, and then tighten the fixing screws after closing. Pay attention to the vertical direction of the reactor body during installation.
5. The stir bar is fixed on the toothed ring chuck of the motor main shaft. The stir bar passes through the middle rotating bearing of the cover, tightens the special connector, and then adjusts the position of the motor, paying attention to the vertical concentricity.
6. The slider on the pole is a stainless steel multi-purpose clamp that adjusts the direction and height in different directions.
7. On the left side of the bottle cap, the 40# standard port plug-in type reflux condenser, the right side 40# is the feeding port connected to the constant pressure funnel, the middle front 24# standard port is inserted into the thermometer casing mouth, and the rear of the hat is the 34# standard port. It is a multi-functional spare port, and the bottom is provided with a discharge valve, and the bottom of the kettle body is respectively a circulating fluid inlet and outlet. The lower port is connected to the circulating fluid inlet, and the upper port is connected to the circulating fluid return port.
8. When installing the glass instrument, it must be cleaned, and the interface should be coated with Vaseline to prevent the glass from locking up, and then apply vacuum grease to prevent air leakage.
9. Press the universal wheel wheel fixing device to stir. If the stirring is stable, the debugging is good.